Experimental Characterization of In-Plane Permeability of Gas Diffusion Layers: Influence of the Saturation Level

Date
2009-05
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University of Delaware
Abstract
Proton Exchange Membrane Fuel Cell or Polymer Electrolyte Membrane Fuel Cell (PEMFC) is a promising energy conversion device due to its clean and efficient operation. Gas Diffusion Layer (GDL), a thin porous material, is one of its key components. It has been shown that by tailoring the GDL properties one can increase the PEMFC performance significantly. Characterizing the material properties is very important for material selection in a design process. The focus of this work is to experimentally measure an important property of the GDL material: permeability (or more specifically in-plane permeability, since the material is typically not isotropic). Water is the byproduct of the fuel cell reaction. During the PEMFC operation, water often condenses within the GDL pores thus hindering the gas flow and blocking the gas access to the reaction sites (catalyst layers). The main goal of our experiments is to measure the influence of the water content within the porous GDL (or, saturation) on the in-plane permeability. Convection is often a key mode of reactant transport, and its influence varies depending on the channel configuration. As the materials are porous, one can use the porous media theory of Darcy’s law to describe the convective transport for which one should first characterize the permeability of the material which is an input required in Darcy’s law which relates the flow rate through a porous material with the pressure drop experienced by the fluid. So convection is important and to model convection, one needs to measure permeability of the GDL. GDL is anisotropic; hence one must characterize in-plane (and through-plane) permeability. Water condenses in the GDL pores, so one must be able to describe permeability as a function of the saturation level. For the purpose of this investigation, the in-plane permeability of the dry GDLs was compared to the in-plane permeability of the wet (i.e. water-saturated) GDL’s for different saturation levels. . For future work, different types GDLs are to be compared to each other in addition to the effect of coating GDL with Teflon, to change the hydrophobicity level of the GDL, and its permeability and saturation level. Findings and results of this project include the measurements for plain carbon paper (TGP-H-060 by Toray Industries, Inc.). Due to several major problems, primarily coming from the complexity of the experimental setup, accruing more reliable data for the above GDL type, as well as comparing the data for different GDL types, has been postponed for the future. During the project, we have encountered several difficulties as follows: Scale malfunction, test stand inaccuracy, a number of hidden leaks in the plumbing of humid air, and condensation of water in the chamber manifolds. All the former problems have been addressed and the only problem left to solve to get very accurate data is to find out where water condenses in the tubes. This would help explaining less water collected at the end of the experiments compare to how much it is put in. The condensation problem is greatly reduced by running experiments with dry inlet air. Exponentially increase of permeability in the beginning of the run could be due to the water being pushed out by force rather than drying over time which is actually desired. Result curves start to smooth out for permeability around 40% saturation and flatten out until GDLs gets dry.
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